Volume 4, Issue 1 (winter & spring 2007 2007)                   IJMSE 2007, 4(1): 48-51 | Back to browse issues page

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B. Alinejad1,, H. Sarpoolaky1,, A. Beitollahi1, S. Afshar2. LOW TEMPERATURE SYNTHESIS OF NANOCRYSTALLINE MgAl2O4 SPINEL VIA SUCROSE PROCESS. IJMSE 2007; 4 (1) :48-51
URL: http://ijmse.iust.ac.ir/article-1-116-en.html
LOW TEMPERATURE SYNTHESIS OF NANOCRYSTALLINE MgAl2O4 SPINEL VIA SUCROSE PROCESS
B. Alinejad1, , H. Sarpoolaky1, , A. Beitollahi1 , S. Afshar2
Abstract:   (28675 Views)
Abstract: Nanocrystalline MgAl2O4 spinel powder was synthesized using metal nitrates and a polymer matrix-based composed of sucrose and polyvinyl alcohol (PVA). The precursor and the calcined powders were characterized by simultaneous thermal analysis (STA), X-ray diffraction (XRD), Fourier transform infrared spectroscopy (FT-IR), and scanning electron microscopy (SEM). According to XRD results, the inceptive formation temperature of spinel via this technique was between 600°C and 700°C. The average crystallite size of calcined powder at 800°C for 2h was in the range of 8-12nm. In addition, SEM micrograph showed that the synthesized powder had a spherical morphology.
Keywords: Spinel- Nanocrystalline- synthesis- polymer matrix
     
Type of Study: Research Paper |
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